Análisis de la influencia de la adición de biosólidos calcinados en la resistencia a la compresión de un mortero

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dc.contributor.advisorPineda Jaimes, Jorge Arturo
dc.contributor.authorRamírez Muñoz, Martín Felipe
dc.contributor.orcidPineda Jaimes, Jorge Arturo [0000-0002-0953-9745]
dc.date.accessioned2025-09-04T20:57:07Z
dc.date.available2025-09-04T20:57:07Z
dc.date.created2025-08-20
dc.descriptionSe estudia la viabilidad de que los biosólidos, provenientes de una planta de tratamiento de aguas residuales (PTAR), sean utilizados como suplemento cementante y sean incinerados a 850 °C. Se prepararon dos tipos de cenizas, diferenciadas por su tiempo de calcinación: BC1 (biosólidos calcinados por sesenta minutos) y BC3 (biosólidos calcinados por ciento ochenta minutos). Ambas fueron incluidas en lugar del 5%, 10%, 15%, 20%, 25% y el 30% de la mezcla de cemento, generando series de probetas cúbicas con dimensiones de 50 mm que se curaron por un lapso de 28 días. Los resultados del ensayo de resistencia a la compresión muestran dos situaciones ideales: 1. BC3 al 5 %, que mejora la resistencia a la compresión hasta los 186 kg/cm² (+52 % en comparación con el control), y 2. BC1 al 30 %, alcanza una resistencia de 218 kg/cm² (+79 % en comparación con el control). El estudio multiescala SEM-EDS (200→2 µm) reveló que la ceniza de 3 horas, la cual es rica en óxidos reactivos de Ca-Si-Al, consume portlandita y produce geles C-S-H/C-A-S-H densos, los cuales tapan el área de transición entre la pasta y el árido. En cambio, la ceniza de 1 hora, con carbono residual, también funciona como agente de curado interno y como filler al llenar capilares a dosificaciones elevadas. Los espectros EDS confirmaron que las mezclas con mejor rendimiento tenían una relación Ca/Si de entre 1.2 y 1.5, así como la existencia de carbón-aluminatos y etringita que fortalecen la matriz.
dc.description.abstractThe feasibility of using biosolids from a wastewater treatment plant (WWTP) as a cementitious supplement and incinerated at 850°C is being studied. Two types of ash were prepared, differentiated by their calcination time: BC1 (biosolids calcined for sixty minutes) and BC3 (biosolids calcined for one hundred and eighty minutes). Both were included in place of 5%, 10%, 15%, 20%, 25%, and 30% of the cement mix, generating series of 50 mm cubic specimens that were cured for a period of 28 days. The compressive strength test results show two ideal situations: 1. BC3 at 5%, which improves the compressive strength to 186 kg/cm² (+52% compared to the control), and 2. BC1 at 30%, reaching a strength of 218 kg/cm² (+79% compared to the control). The multiscale SEM-EDS study (200→2 µm) revealed that the 3-hour ash, which is rich in reactive Ca-Si-Al oxides, consumes portlandite and produces dense C-S-H/C-A-S-H gels, which obscure the transition area between the paste and the aggregate. In contrast, the 1-hour ash, with residual carbon, also functions as an internal curing agent and as a filler by filling capillaries at high dosages. EDS spectra confirmed that the best-performing mixtures had a Ca/Si ratio between 1.2 and 1.5, as well as the presence of carbon-aluminates and ettringite that strengthen the matrix.
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dc.identifier.urihttp://hdl.handle.net/11349/98812
dc.language.isospa
dc.publisherUniversidad Distrital Francisco José de Caldas
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dc.rights.accesoAbierto (Texto Completo)
dc.rights.accessrightsOpenAccess
dc.subjectAnálisis microestructural SEM-EDS
dc.subjectBiosólidos calcinados
dc.subjectMaterial cementante suplementario
dc.subjectMortero sostenible
dc.subjectReactividad puzolánica
dc.subjectResistencia a la compresión
dc.subject.keywordSEM-EDS microstructural analysis
dc.subject.keywordCalcined biosolids
dc.subject.keywordSupplementary cementitious material
dc.subject.keywordSustainable mortar
dc.subject.keywordPozzolanic reactivity
dc.subject.keywordCompressive strength
dc.subject.lembMaestría en Ingeniería Civil -- Tesis y disertaciones académicas
dc.subject.lembMateriales de construcción
dc.subject.lembCemento
dc.subject.lembResistencia de materiales
dc.subject.lembPurificación de aguas residuales
dc.titleAnálisis de la influencia de la adición de biosólidos calcinados en la resistencia a la compresión de un mortero
dc.title.titleenglishAnalysis of the influence of the addition of calcined biosolids on the compressive strength of a mortar
dc.typemasterThesis
dc.type.coarhttp://purl.org/coar/resource_type/c_bdcc
dc.type.degreeInvestigación-Innovación
dc.type.driverinfo:eu-repo/semantics/masterThesis

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